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采用真空电弧炉熔炼并制备等原子比的HfNbZrTiTa高熵合金。通过XRD、SEM、EDS、电子万能试验机和霍普金森压杆对合金的显微组织、室温准静态压缩性能及室温(298 K)、低温(77 K)下的动态压缩性能进行研究。结果表明:该合金显微组织主要为BCC固溶体结构,晶间存在少量共晶组织;具有良好的塑性,室温下压缩塑性超50%且未发生断裂;HfNbZrTiTa合金在动态压缩试验条件下(应变速率为2 000~4 000 s-1),材料应变敏感性较低;当温度从298 K降到77 K,流变应力变化不明显。
Abstract:HfNbZrTiTa high entropy alloy with equal atomic ratio was prepared by vacuum arc furnace melting.The microstructure, quasi-static compression properties at room temperature and dynamic compression properties at room temperature(298 K)and low temperature(77 K)were studied by XRD,SEM,EDS,electronic universal testing machine and Hopkinson pressure bar tester.The results show that the microstructure of the alloy is mainly BCC solid solution structure, there is a small amount of eutectic structure between the grains, and it has good plasticity.The compression plasticity at room temperature exceeds 50% without fracture.In the dynamic compression test, the strain rate is controlled in the range of 2 000 to 4 000 s-1.When the temperature drops from 298 K to 77 K,the flow stress change is not obvious.
[1] LILENSTEN L,COUZINIé J P,PERRIèRE L,et al.Study of a bcc multi-principal element alloy:tensile and simple shear properties and underlying deformation mechanisms[J].Acta Materialia,2018,142:131-141.
[2] KIM I H,OH H S,LEE K S,et al.Optimization of conflicting properties via engineering compositional complexity in refractory high entropy alloys[J].Scripta Materialia,2021,199:113839.
[3] SHAHMIR H,ASGHARI-RAD P,MEHRANPOUR M S,et al.Evidence of FCC to HCP and BCC-martensitic transformations in a CoCrFeNiMn high-entropy alloy by severe plastic deformation[J].Materials Science and Engineering A,2021,807:140875.
[4] 王夺,李文,付华萌.CoCrFeNiCu2Snx高熵合金的微观组织与性能[J].沈阳理工大学学报,2014,33(4):30-33.WANG D,LI W,FU H M.The microstructure and properties of CoCrFeNiCu2Snx high-entropy alloys[J].Journal of Shenyang Ligong University,2014,33(4):30-33.(in Chinese)
[5] SENKOV O N,GORSSE S,MIRACLE D B.High temperature strength of refractory complex concentrated alloys[J].Acta Materialia,2019,175:394-405.
[6] WU S Y,QIAO D X,ZHANG H T,et al.Microstructure and mechanical properties of CxHf0.25NbTaW0.5 refractory high-entropy alloys at room and high temperatures[J].Journal of Materials Science & Technology,2022,97:229-238.
[7] HUANG W J,WANG X J,QIAO J W,et al.Microstructures and mechanical properties of TiZrHfNbTaWx refractory high entropy alloys[J].Journal of Alloys and Compounds,2022,914:165187.
[8] 高炜,余竹焕,阎亚雯,等.Cr对FeCoNiAlCrx高熵合金组织与力学性能的影响[J].材料工程,2023,51(2):91-97.GAO W,YU Z H,YAN Y W,et al.Effect of Cr on microstructure and mechanical properties of FeCoNiAlCrx high entropy alloys[J].Journal of Materials Engineering,2023,51(2):91-97.(in Chinese)
[9] 曾琪皓,张松,胥永刚,等.Hf含量对NbMo0.5HfxTiZrCrAl难熔高熵合金组织及力学性能的影响[J].稀有金属材料与工程,2022,51(3):1024-1030.ZENG Q H,ZHANG S,XU Y G,et al.Effects of Hf content on microstructure and mechanical properties of NbMo0.5HfxTiZrCrAl refractory high-entropy alloy[J].Rare Metal Materials and Engineering,2022,51(3):1024-1030.(in Chinese)
[10] SONG W L,MA Q,ZENG Q L,et al.Experimental and numerical study on the dynamic shear banding mechanism of HfNbZrTi high entropy alloy[J].Science China Technological Sciences,2022,65(8):1808-1818.
[11] 王开心,仝永刚,陈永雄,等.高熵合金动态力学行为研究进展[J].材料工程,2024,52(1):57-69.WANG K X,TONG Y G,CHEN Y X,et al.Research progress in dynamic mechanical behavior of high-entropy alloys[J].Journal of Materials Engineering,2024,52(1):57-69.(in Chinese)
[12] HE Q F,WANG J G,CHEN H A,et al.A highly distorted ultraelastic chemically complex Elinvar alloy[J].Nature,2022,602(7896):251-257.
[13] ZHANG F X,SONG H Q.Effect of atomic size mismatch and chemical complexity on the local lattice distortion of BCC solid solution alloys[J].Materials Today Communications,2022,33:104367.
[14] LI J,CHEN Y,HE Q F,et al.Heterogeneous lattice strain strengthening in severely distorted crystalline solids[J].Proceedings of the National Academy of Sciences of the United States of America,2022,119(25):e2200607119.
[15] CHEN X F,WANG Q,CHENG Z Y,et al.Direct observation of chemical short-range order in a medium-entropy alloy[J].Nature,2021,592(7856):712-716.
[16] ZHANG R P,ZHAO S T,DING J,et al.Short-range order and its impact on the CrCoNi medium-entropy alloy[J].Nature,2020,581:283-287.
[17] LI Q J,SHENG H,MA E.Strengthening in multi-principal element alloys with local-chemical-order roughened dislocation pathways[J].Nature Communications,2019,10:3563.
[18] SHI P J,REN W L,ZHENG T X,et al.Enhanced strength-ductility synergy in ultrafine-grained eutectic high-entropy alloys by inheriting microstructural lamellae[J].Nature Communications,2019,10(1):489.
[19] LI Y,LI W,LI S L,et al.Ensuring the strength and ductility synergy in an austenitic stainless steel:single-or multi-phase hetero-structures design[J].Scripta Materialia,2021,193:81-85.
[20] LI Y,LU Y F,LI W,et al.Hierarchical microstructure design of a bimodal grained twinning-induced plasticity steel with excellent cryogenic mechanical properties[J].Acta Materialia,2018,158:79-94.
[21] SENKOV O N,SCOTT J M,SENKOVA S V,et al.Microstructure and room temperature properties of a high-entropy TaNbHfZrTi alloy[J].Journal of Alloys and Compounds,2011,509(20):6043-6048.
基本信息:
中图分类号:TG139
引用信息:
[1]魏韬,张伟强,张丽,等.HfNbZrTiTa高熵合金的组织与压缩性能[J].沈阳理工大学学报,2025,44(02):73-78+85.
基金信息:
辽宁省教育厅高等学校基本科研项目(LJKMZ20220592)
2025-02-26
2025-02-26